Design of Nickel Supported on Water-Tolerant Nb2O5 Catalysts for the Hydrotreating of Lignin Streams Obtained from Lignin-First Biorefining.
Identifieur interne : 000A37 ( Main/Exploration ); précédent : 000A36; suivant : 000A38Design of Nickel Supported on Water-Tolerant Nb2O5 Catalysts for the Hydrotreating of Lignin Streams Obtained from Lignin-First Biorefining.
Auteurs : Glauco F. Leal [Brésil] ; Sérgio Lima [Royaume-Uni] ; Inês Graça [Royaume-Uni] ; Heloise Carrer [Brésil] ; Dean H. Barrett [Afrique du Sud] ; Erico Teixeira-Neto [Brésil] ; Antonio Aprigio S. Curvelo [Brésil] ; Cristiane B. Rodella [Brésil] ; Roberto Rinaldi [Royaume-Uni]Source :
- iScience [ 2589-0042 ] ; 2019.
Abstract
In biomass conversion, Nb2O5 has attracted increasing attention as a catalyst support presenting water-tolerant Lewis acid sites. Herein, we address the design of Ni/Nb2O5 catalysts for hydrotreating of lignin to hydrocarbons. To optimize the balance between acidic and hydrogenating properties, the catalysts were first evaluated in the hydrotreating of diphenyl ether. The best catalyst candidate was further explored in the conversion of lignin oil obtained by catalytic upstream biorefining of poplar. As primary products, cycloalkanes were obtained, demonstrating the potential of Ni/Nb2O5 catalysts for the lignin-to-fuels route. However, the Lewis acidity of Nb2O5 also catalyzes coke formation via lignin species condensation. Thereby, an acidity threshold should be found so that dehydration reactions essential to the hydrotreatment are not affected, but the condensation of lignin species prevented. This article provides a critical "beginning-to-end" analysis of aspects crucial to the catalyst design to produce lignin biofuels.
DOI: 10.1016/j.isci.2019.05.007
PubMed: 31125909
PubMed Central: PMC6532020
Affiliations:
- Afrique du Sud, Brésil, Royaume-Uni
- Gauteng, État de São Paulo
- Johannesbourg, São Paulo
- Université de São Paulo, Université du Witwatersrand
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Leal</name><affiliation wicri:level="4"><nlm:affiliation>Department of Chemical Engineering, Imperial College London, South Kensington Campus, London SW7 2AZ, UK; Department of Physical Chemistry, Institute of Chemistry of São Carlos, University of São Paulo, Av. Trabalhador São Carlense, 400, São Carlos, São Paulo 13566-590, Brazil; Brazilian Synchrotron Light Laboratory (LNLS), Brazilian Center for Research in Energy and Materials (CNPEM), Campinas, São Paulo 13083-970, Brazil.</nlm:affiliation><country xml:lang="fr">Brésil</country><wicri:regionArea>Department of Chemical Engineering, Imperial College London, South Kensington Campus, London SW7 2AZ, UK; Department of Physical Chemistry, Institute of Chemistry of São Carlos, University of São Paulo, Av. Trabalhador São Carlense, 400, São Carlos, São Paulo 13566-590, Brazil; Brazilian Synchrotron Light Laboratory (LNLS), Brazilian Center for Research in Energy and Materials (CNPEM), Campinas, São Paulo 13083-970</wicri:regionArea><placeName><settlement type="city">São Paulo</settlement><region type="state">État de São Paulo</region></placeName><orgName type="university">Université de São Paulo</orgName><placeName><settlement type="city">São Paulo</settlement><region type="state">État de São Paulo</region></placeName></affiliation></author><author><name sortKey="Lima, Sergio" sort="Lima, Sergio" uniqKey="Lima S" first="Sérgio" last="Lima">Sérgio Lima</name><affiliation wicri:level="1"><nlm:affiliation>Department of Chemical Engineering, Imperial College London, South Kensington Campus, London SW7 2AZ, UK.</nlm:affiliation><country xml:lang="fr">Royaume-Uni</country><wicri:regionArea>Department of Chemical Engineering, Imperial College London, South Kensington Campus, London SW7 2AZ</wicri:regionArea><wicri:noRegion>London SW7 2AZ</wicri:noRegion></affiliation></author><author><name sortKey="Graca, Ines" sort="Graca, Ines" uniqKey="Graca I" first="Inês" last="Graça">Inês Graça</name><affiliation wicri:level="1"><nlm:affiliation>Department of Chemical Engineering, Imperial College London, South Kensington Campus, London SW7 2AZ, UK.</nlm:affiliation><country xml:lang="fr">Royaume-Uni</country><wicri:regionArea>Department of Chemical Engineering, Imperial College London, South Kensington Campus, London SW7 2AZ</wicri:regionArea><wicri:noRegion>London SW7 2AZ</wicri:noRegion></affiliation></author><author><name sortKey="Carrer, Heloise" sort="Carrer, Heloise" uniqKey="Carrer H" first="Heloise" last="Carrer">Heloise Carrer</name><affiliation wicri:level="1"><nlm:affiliation>Brazilian Synchrotron Light Laboratory (LNLS), Brazilian Center for Research in Energy and Materials (CNPEM), Campinas, São Paulo 13083-970, Brazil.</nlm:affiliation><country xml:lang="fr">Brésil</country><wicri:regionArea>Brazilian Synchrotron Light Laboratory (LNLS), Brazilian Center for Research in Energy and Materials (CNPEM), Campinas, São Paulo 13083-970</wicri:regionArea><placeName><settlement type="city">São Paulo</settlement><region type="state">État de São Paulo</region></placeName></affiliation></author><author><name sortKey="Barrett, Dean H" sort="Barrett, Dean H" uniqKey="Barrett D" first="Dean H" last="Barrett">Dean H. Barrett</name><affiliation wicri:level="4"><nlm:affiliation>Brazilian Synchrotron Light Laboratory (LNLS), Brazilian Center for Research in Energy and Materials (CNPEM), Campinas, São Paulo 13083-970, Brazil; School of Chemistry, University of the Witwatersrand, Johannesburg, South Africa.</nlm:affiliation><country xml:lang="fr">Afrique du Sud</country><wicri:regionArea>Brazilian Synchrotron Light Laboratory (LNLS), Brazilian Center for Research in Energy and Materials (CNPEM), Campinas, São Paulo 13083-970, Brazil; School of Chemistry, University of the Witwatersrand, Johannesburg</wicri:regionArea><orgName type="university">Université du Witwatersrand</orgName><placeName><settlement type="city">Johannesbourg</settlement><region type="region" nuts="2">Gauteng</region></placeName></affiliation></author><author><name sortKey="Teixeira Neto, Erico" sort="Teixeira Neto, Erico" uniqKey="Teixeira Neto E" first="Erico" last="Teixeira-Neto">Erico Teixeira-Neto</name><affiliation wicri:level="1"><nlm:affiliation>Brazilian Nanotechnology National Laboratory (LNNano), Brazilian Center for Research in Energy and Materials (CNPEM), Campinas, São Paulo 13083-970, Brazil.</nlm:affiliation><country xml:lang="fr">Brésil</country><wicri:regionArea>Brazilian Nanotechnology National Laboratory (LNNano), Brazilian Center for Research in Energy and Materials (CNPEM), Campinas, São Paulo 13083-970</wicri:regionArea><placeName><settlement type="city">São Paulo</settlement><region type="state">État de São Paulo</region></placeName></affiliation></author><author><name sortKey="Curvelo, Antonio Aprigio S" sort="Curvelo, Antonio Aprigio S" uniqKey="Curvelo A" first="Antonio Aprigio S" last="Curvelo">Antonio Aprigio S. Curvelo</name><affiliation wicri:level="4"><nlm:affiliation>Department of Physical Chemistry, Institute of Chemistry of São Carlos, University of São Paulo, Av. Trabalhador São Carlense, 400, São Carlos, São Paulo 13566-590, Brazil.</nlm:affiliation><country xml:lang="fr">Brésil</country><wicri:regionArea>Department of Physical Chemistry, Institute of Chemistry of São Carlos, University of São Paulo, Av. Trabalhador São Carlense, 400, São Carlos, São Paulo 13566-590</wicri:regionArea><placeName><settlement type="city">São Paulo</settlement><region type="state">État de São Paulo</region></placeName><orgName type="university">Université de São Paulo</orgName><placeName><settlement type="city">São Paulo</settlement><region type="state">État de São Paulo</region></placeName></affiliation></author><author><name sortKey="Rodella, Cristiane B" sort="Rodella, Cristiane B" uniqKey="Rodella C" first="Cristiane B" last="Rodella">Cristiane B. Rodella</name><affiliation wicri:level="1"><nlm:affiliation>Brazilian Synchrotron Light Laboratory (LNLS), Brazilian Center for Research in Energy and Materials (CNPEM), Campinas, São Paulo 13083-970, Brazil.</nlm:affiliation><country xml:lang="fr">Brésil</country><wicri:regionArea>Brazilian Synchrotron Light Laboratory (LNLS), Brazilian Center for Research in Energy and Materials (CNPEM), Campinas, São Paulo 13083-970</wicri:regionArea><placeName><settlement type="city">São Paulo</settlement><region type="state">État de São Paulo</region></placeName></affiliation></author><author><name sortKey="Rinaldi, Roberto" sort="Rinaldi, Roberto" uniqKey="Rinaldi R" first="Roberto" last="Rinaldi">Roberto Rinaldi</name><affiliation wicri:level="1"><nlm:affiliation>Department of Chemical Engineering, Imperial College London, South Kensington Campus, London SW7 2AZ, UK. Electronic address: rrinaldi@ic.ac.uk.</nlm:affiliation><country xml:lang="fr">Royaume-Uni</country><wicri:regionArea>Department of Chemical Engineering, Imperial College London, South Kensington Campus, London SW7 2AZ</wicri:regionArea><wicri:noRegion>London SW7 2AZ</wicri:noRegion></affiliation></author></analytic><series><title level="j">iScience</title><idno type="eISSN">2589-0042</idno><imprint><date when="2019" type="published">2019</date></imprint></series></biblStruct></sourceDesc></fileDesc><profileDesc><textClass></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">In biomass conversion, Nb<sub>2</sub>O<sub>5</sub> has attracted increasing attention as a catalyst support presenting water-tolerant Lewis acid sites. Herein, we address the design of Ni/Nb<sub>2</sub>O<sub>5</sub> catalysts for hydrotreating of lignin to hydrocarbons. To optimize the balance between acidic and hydrogenating properties, the catalysts were first evaluated in the hydrotreating of diphenyl ether. The best catalyst candidate was further explored in the conversion of lignin oil obtained by catalytic upstream biorefining of poplar. As primary products, cycloalkanes were obtained, demonstrating the potential of Ni/Nb<sub>2</sub>O<sub>5</sub> catalysts for the lignin-to-fuels route. However, the Lewis acidity of Nb<sub>2</sub>O<sub>5</sub> also catalyzes coke formation via lignin species condensation. Thereby, an acidity threshold should be found so that dehydration reactions essential to the hydrotreatment are not affected, but the condensation of lignin species prevented. This article provides a critical "beginning-to-end" analysis of aspects crucial to the catalyst design to produce lignin biofuels.</div></front></TEI><pubmed><MedlineCitation Status="PubMed-not-MEDLINE" Owner="NLM"><PMID Version="1">31125909</PMID><DateRevised><Year>2020</Year><Month>10</Month><Day>01</Day></DateRevised><Article PubModel="Print-Electronic"><Journal><ISSN IssnType="Electronic">2589-0042</ISSN><JournalIssue CitedMedium="Internet"><Volume>15</Volume><PubDate><Year>2019</Year><Month>May</Month><Day>31</Day></PubDate></JournalIssue><Title>iScience</Title><ISOAbbreviation>iScience</ISOAbbreviation></Journal><ArticleTitle>Design of Nickel Supported on Water-Tolerant Nb<sub>2</sub>O<sub>5</sub> Catalysts for the Hydrotreating of Lignin Streams Obtained from Lignin-First Biorefining.</ArticleTitle><Pagination><MedlinePgn>467-488</MedlinePgn></Pagination><ELocationID EIdType="pii" ValidYN="Y">S2589-0042(19)30144-0</ELocationID><ELocationID EIdType="doi" ValidYN="Y">10.1016/j.isci.2019.05.007</ELocationID><Abstract><AbstractText>In biomass conversion, Nb<sub>2</sub>O<sub>5</sub> has attracted increasing attention as a catalyst support presenting water-tolerant Lewis acid sites. Herein, we address the design of Ni/Nb<sub>2</sub>O<sub>5</sub> catalysts for hydrotreating of lignin to hydrocarbons. To optimize the balance between acidic and hydrogenating properties, the catalysts were first evaluated in the hydrotreating of diphenyl ether. The best catalyst candidate was further explored in the conversion of lignin oil obtained by catalytic upstream biorefining of poplar. As primary products, cycloalkanes were obtained, demonstrating the potential of Ni/Nb<sub>2</sub>O<sub>5</sub> catalysts for the lignin-to-fuels route. However, the Lewis acidity of Nb<sub>2</sub>O<sub>5</sub> also catalyzes coke formation via lignin species condensation. Thereby, an acidity threshold should be found so that dehydration reactions essential to the hydrotreatment are not affected, but the condensation of lignin species prevented. This article provides a critical "beginning-to-end" analysis of aspects crucial to the catalyst design to produce lignin biofuels.</AbstractText><CopyrightInformation>Copyright © 2019 The Author(s). Published by Elsevier Inc. All rights reserved.</CopyrightInformation></Abstract><AuthorList CompleteYN="Y"><Author ValidYN="Y"><LastName>Leal</LastName><ForeName>Glauco F</ForeName><Initials>GF</Initials><AffiliationInfo><Affiliation>Department of Chemical Engineering, Imperial College London, South Kensington Campus, London SW7 2AZ, UK; Department of Physical Chemistry, Institute of Chemistry of São Carlos, University of São Paulo, Av. Trabalhador São Carlense, 400, São Carlos, São Paulo 13566-590, Brazil; Brazilian Synchrotron Light Laboratory (LNLS), Brazilian Center for Research in Energy and Materials (CNPEM), Campinas, São Paulo 13083-970, Brazil.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Lima</LastName><ForeName>Sérgio</ForeName><Initials>S</Initials><AffiliationInfo><Affiliation>Department of Chemical Engineering, Imperial College London, South Kensington Campus, London SW7 2AZ, UK.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Graça</LastName><ForeName>Inês</ForeName><Initials>I</Initials><AffiliationInfo><Affiliation>Department of Chemical Engineering, Imperial College London, South Kensington Campus, London SW7 2AZ, UK.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Carrer</LastName><ForeName>Heloise</ForeName><Initials>H</Initials><AffiliationInfo><Affiliation>Brazilian Synchrotron Light Laboratory (LNLS), Brazilian Center for Research in Energy and Materials (CNPEM), Campinas, São Paulo 13083-970, Brazil.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Barrett</LastName><ForeName>Dean H</ForeName><Initials>DH</Initials><AffiliationInfo><Affiliation>Brazilian Synchrotron Light Laboratory (LNLS), Brazilian Center for Research in Energy and Materials (CNPEM), Campinas, São Paulo 13083-970, Brazil; School of Chemistry, University of the Witwatersrand, Johannesburg, South Africa.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Teixeira-Neto</LastName><ForeName>Erico</ForeName><Initials>E</Initials><AffiliationInfo><Affiliation>Brazilian Nanotechnology National Laboratory (LNNano), Brazilian Center for Research in Energy and Materials (CNPEM), Campinas, São Paulo 13083-970, Brazil.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Curvelo</LastName><ForeName>Antonio Aprigio S</ForeName><Initials>AAS</Initials><AffiliationInfo><Affiliation>Department of Physical Chemistry, Institute of Chemistry of São Carlos, University of São Paulo, Av. Trabalhador São Carlense, 400, São Carlos, São Paulo 13566-590, Brazil.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Rodella</LastName><ForeName>Cristiane B</ForeName><Initials>CB</Initials><AffiliationInfo><Affiliation>Brazilian Synchrotron Light Laboratory (LNLS), Brazilian Center for Research in Energy and Materials (CNPEM), Campinas, São Paulo 13083-970, Brazil.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Rinaldi</LastName><ForeName>Roberto</ForeName><Initials>R</Initials><AffiliationInfo><Affiliation>Department of Chemical Engineering, Imperial College London, South Kensington Campus, London SW7 2AZ, UK. Electronic address: rrinaldi@ic.ac.uk.</Affiliation></AffiliationInfo></Author></AuthorList><Language>eng</Language><PublicationTypeList><PublicationType UI="D016428">Journal Article</PublicationType></PublicationTypeList><ArticleDate DateType="Electronic"><Year>2019</Year><Month>05</Month><Day>09</Day></ArticleDate></Article><MedlineJournalInfo><Country>United States</Country><MedlineTA>iScience</MedlineTA><NlmUniqueID>101724038</NlmUniqueID><ISSNLinking>2589-0042</ISSNLinking></MedlineJournalInfo><KeywordList Owner="NOTNLM"><Keyword MajorTopicYN="N">Biofuel</Keyword><Keyword MajorTopicYN="N">Catalysis</Keyword><Keyword MajorTopicYN="N">Energy Materials</Keyword></KeywordList></MedlineCitation><PubmedData><History><PubMedPubDate PubStatus="received"><Year>2018</Year><Month>12</Month><Day>13</Day></PubMedPubDate><PubMedPubDate PubStatus="revised"><Year>2019</Year><Month>04</Month><Day>29</Day></PubMedPubDate><PubMedPubDate 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21;12(6):1203-1212</Citation><ArticleIdList><ArticleId IdType="pubmed">30673171</ArticleId></ArticleIdList></Reference></ReferenceList></PubmedData></pubmed><affiliations><list><country><li>Afrique du Sud</li><li>Brésil</li><li>Royaume-Uni</li></country><region><li>Gauteng</li><li>État de São Paulo</li></region><settlement><li>Johannesbourg</li><li>São Paulo</li></settlement><orgName><li>Université de São Paulo</li><li>Université du Witwatersrand</li></orgName></list><tree><country name="Brésil"><region name="État de São Paulo"><name sortKey="Leal, Glauco F" sort="Leal, Glauco F" uniqKey="Leal G" first="Glauco F" last="Leal">Glauco F. Leal</name></region><name sortKey="Carrer, Heloise" sort="Carrer, Heloise" uniqKey="Carrer H" first="Heloise" last="Carrer">Heloise Carrer</name><name sortKey="Curvelo, Antonio Aprigio S" sort="Curvelo, Antonio Aprigio S" uniqKey="Curvelo A" first="Antonio Aprigio S" last="Curvelo">Antonio Aprigio S. Curvelo</name><name sortKey="Rodella, Cristiane B" sort="Rodella, Cristiane B" uniqKey="Rodella C" first="Cristiane B" last="Rodella">Cristiane B. Rodella</name><name sortKey="Teixeira Neto, Erico" sort="Teixeira Neto, Erico" uniqKey="Teixeira Neto E" first="Erico" last="Teixeira-Neto">Erico Teixeira-Neto</name></country><country name="Royaume-Uni"><noRegion><name sortKey="Lima, Sergio" sort="Lima, Sergio" uniqKey="Lima S" first="Sérgio" last="Lima">Sérgio Lima</name></noRegion><name sortKey="Graca, Ines" sort="Graca, Ines" uniqKey="Graca I" first="Inês" last="Graça">Inês Graça</name><name sortKey="Rinaldi, Roberto" sort="Rinaldi, Roberto" uniqKey="Rinaldi R" first="Roberto" last="Rinaldi">Roberto Rinaldi</name></country><country name="Afrique du Sud"><region name="Gauteng"><name sortKey="Barrett, Dean H" sort="Barrett, Dean H" uniqKey="Barrett D" first="Dean H" last="Barrett">Dean H. Barrett</name></region></country></tree></affiliations></record>Pour manipuler ce document sous Unix (Dilib)
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